Chapter 1 Introduction of Experimental Organic Chemistry 1.1 The Role of Experimental Organic Chemistry 1.2 General Rules for the Organic Chemistry Experiments 1.3 Safety in the Organic Chemistry Laboratory 1.4 Pre-lab Reports.Notebooks and Lab Reports in the Laboratory 1.5 Common Laboratory Glassware and Equipment 1.6 The Literature of Organic Chemistry 1.7 Green Chemistry in the Organic Laboratory Chapter 2 Basic Operations of Organic Chemistry Experiments 2.1 Heating and Cooling 2.2 Drying Organic Solutions and Solids 2.3 Filtration 2.4 Simple Distillation and Boiling Point 2.5 Fractional Distillation 2.6 Steam Distillation 2.7 Vacuum Distillation 2.8 Extraction and Washing 2.9 Recrystallization 2.10 Sublimation 2.11 Measurement of the Melting Point 2.12 Refluxing 2.13 Stirring Methods 2.14 Water-free and Air-free Operation 2.15 Chromatography Techniques Chapter 3 Fundamental Experiments 3.1 Unsaturated Hydrocarbons Exp.1 Preparation of Cyclohexene Exp.2 Preparation of Phenylacetylene 3.2 Alkyl Halides Exp.3 Preparation of 1-Bromobutane Exp.4 Preparation of 2 Chloro 2 methylbutane 3.3 Alcohols，Phenols and Ethers Exp.5 Preparation of 2-Methyl-2-butanol Exp.6 Preparation of Triphenylmethanol Exp.7 Preparation of Di n-butyl Ether Exp.8 Preparation of Ethyl Phenyl Ether Exp.9 Preparation of o-tert Butylhydroquinone 3.4 Aldehydes and Ketones Exp.10 Preparation of Cyclohexanone Exp.11 Preparation of Acetophenone Exp.12 Preparation of Benzaldehyde 3.5 Carboxylic Acids Exp.13 Preparation of Benzoic Acid Exp.14 Preparation of Cinnamic Acid Exp.15 Preparation of Hexane-1，6 dionic Acid 3.6 Carboxylic Acid Derivatives Exp.16 Preparation of Ethyl Acetate Exp.17 Preparation of nDibutyl Phthalate 3.7 Nitrogen-containing Compounds Exp.18 Preparation of Acetanilide
Exp.19 Preparation of Methyl Orange 3.8 Heterocyclic Compounds Exp.20 Preparation of 8-Hydroxyquinoline Exp.21 Extraction and Separation of Caffeine from Tea Leaves Chapter 4 Comprehensive Experiments Exp.1 Preparation of Benzyl Alcohol and Benzoic Acid Exp.2 Preparation of Benzil and Thin-layer Chromatography Exp.3 Preparation of Acetylferrocene and Column Chromatography Exp.4 Preparation of Ethyl Acetoacetate by the Claisen Condensation Reaction Exp.5 Synthesis and Characterization of Aspirin Exp.6 Multi-step Synthesis of Sulfanilamide Exp.7 A Solvent Free Cannizzaro Reaction and Thin-layer Chromatography Exp.8 Preparation of 4-Vinylbenzoic Acid by a Wittig Reaction Exp.9 Preparation of Dimedone via the Robinson Annulation Exp.10 Preparation of Cinnamic Acid by the Knoevenagel Condensation Exp.11 Microwave assisted Preparation of Benzoic Acid and Ethyl Benzoate Chapter 5 Experiments from Research and Literature Exp.1 Synthesis of 3-Substituted Isoindolin-1-ones by Solvent-free Grinding Reaction Exp.2 Electroorganic Synthesis of Nitriles Exp.3 Ultrasonic Assisted Green Protocol for the Synthesis of N，N-bis Phenylsulfamide Exp.4 Clean Synthesis in Water：Uncatalysed Preparation of Ylidenemalononitriles Exp.5 Transition metal-catalyzed Convenient Synthesis of Internal Alkyne Exp.6 N-Heterocyclic Carbene Catalyzed Intramolecular Benzoin Condensation to Access 9，10-Phenanthraquinone Exp.7 Optical Resolution of （★）（S）-Methyl-（S）phenylsulfoximine with （+）-L-Camphorsulfonic Acid Exp.8 Synthesis of Benzyl Acetate in Room Temperature lonic Liquids Exp.9 Green Synthesis of 4-Bromoaniline Exp.10 Pinacol Rearrangement and Photochemical Synthesis of Benzopinacol Chapter 6 Study Guide of Some Typical Experiments Exp.1 Preparation of Cyclohexene （Miniscale Reaction） Exp.2 Preparation of.1 -Bromobutane Exp.3 Preparation of Acetyl Ferrocene and Column Chromatography Exp.4 Preparation of Acetylaniline Exp.5 Preparation of 2-Methyl2-butanol Exp.6 Preparation of Benzil and Thin-layer Chromatography Exp.7 Preparation of Cinnamic Acid Exp.8 Preparation of Benzoic Acid and Ethyl Benzoate Exp.9 Preparation of Benzoic Acid and Benzyl Alcohol Appendix References
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